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View Full Version : Making Bubble With Ice ~ c-ray stylee


c-ray
09-06-2008, 07:50 PM
*sorry I have no pics to accompany this diatribe, the camera is mia

so recently I have been making bubs using finely crushed ice without adding any water in the mixing stage, only adding water when it is time to use the bags

here's a description of the process

I load the freezer up with plastic containers of water and when it is ice I put it all in a grain bag, pillowcase or what have you and smash that on the concrete with a big hammer until it is fairly well crushed, takes about a minute of some good beating
I dump the crushed ice into a rubbermaid container http://hearthandhomemaker.typepad.com/hearth_and_homemaker/images/2007/11/14/rubbermaid_tote_2.jpg
I grab the material to be processed from the freezer and sprinkle it on top of the ice, I have been using about 2 to 4 times as much ice as shake by volume
I proceed to shake the rubbermaid back and forth, up and down, see saw like and in a back and forth circular motion, anything goes here,...it is a bit of work but it is also a good upper body exercise! :yay: lots of twisting involved, put on some tunes and get into it
when I start to see some water melting and bubbles on the ice that is a sign it is time to rinse the material through ze bubble bags, so I proceed to dump everything from the rubbermaid into some 5 gallon bags that are already to go in a 5 gallon bucket
now I will add some water, enough to cover the material, and then mix it around a bit to help free some trichomes
then I wait until the ice is mostly melted, 15 or so minutes is usually adequate, and then I pull the bags one by one and hang them on a pole...the 220 bag I will squeeze to get lots of the water out but I don't wring the bags or apply excessive force...I dump the shake from the 220 bag into a shopping bag and put it into the fridge to keep it cool until the next run, which should precede as soon as possible, ideally within 24 hours...also after I pull each bag I like to swing it around windmill style real fast to help release the last bits of water, like a human powered centrifuge
I use a plastic spoon with a fine edge, or sometimes a good plastic spatula, to carefully scrape the hash from each bag and I lightly smear it onto a sheet of tyvek to dry...tyvek works great and hash peels from it very easily especially the melty strains that are problematic with cardboard... also it is good idea to put some cardboard under the tyvek to help absorb water that drips through the tyvek...tyvek has small pores like 1 micron...you can get tyvek envelopes for free from fedex dropoff points like kinkos, staples, office depot, etc.
I like to crumble the hash lightly with my fingertips as it is drying to help break it up into finer particles, and I will feel my skin actually absorb some of the moisture from the hash while I am doing this..with the real melty strains it is not possible to do this or receommended because it just mucks them up but it is a good idea to use a nice sharp razor blade to chop into lines about 1mm wide
when the hash is dry, in about a week or something, I take it and pour into some vials I got from a laboratory supply place, you can also find them at head shops but they are cheaper from the lab supply..that is about it



some ideas

I have started using ice only during mixing because I believe that water will oxidize and degrade the essential oils (flavour components) in the hash, so the best idea is to limit the amount of contact with water as much as possible..also the amount of water, the length of time and the temperature of the water in contact with the shake are factors that contribute to rapidly declining quality of hash, especially when multiple runs are taken...also I find that using a lot of ice creates a lot more trichome-ice interaction and I can get better extraction rates than I previously got with other methods, and the quality is higher..I did a test recently a found minimal green in the 3rd run, I will run the material a 4th time to see what the colour looks like but also check it under the microscope to see if there is any significant green matter

it is a good idea to crush the ice as finely as possible, and an even better idea to pour the crushed ice through some 1/2" or 1/4" hardware cloth and return the big chunks to the bag for further smashing...here the theory is that when it is time to put the shake through the bubble bags all the ice will melt in a relatively short time because they are all very small pieces, also smaller ice will have more surface area and random surfaces to contact the shake and it will be smaller so it will be able to get into smaller crevices in the shake

for $100 I could probably build a mechanized seesaw for the rubbermaid to sit on..I could even use a large rubbermaid like 28+ gallons to process multi lbs of shake at a time if necessary

that is about it, I have probably missed something..hope this is helpful for some folks

vapor
09-06-2008, 08:16 PM
sounds fun! i am gona try this soon thanks!

c-ray
09-06-2008, 08:21 PM
do it up!!

vapor
09-06-2008, 08:36 PM
i needs to get me a hippie to do the mixin!

guest
09-06-2008, 08:44 PM
yes Iah!
Nice going C-Man!

I love how you dissect a problem.
One.

purplehaze2
09-06-2008, 08:54 PM
Im ready for a good work out.

EmeraldDreams
09-13-2008, 05:51 AM
Wow!!! Major kudos for this post. Ill definitely try this the next time around. Im totally diggin the workout part too. :laugh2:

guest
09-14-2008, 06:18 AM
nice how-to C :)

*sorry I have no pics to accompany this diatribe, the camera is mia


I guess that means your process works! Can't even find your camera, lol. I'm definlity trying this "soon"...sigh.

later

Microbeman
09-15-2008, 06:33 PM
??

c-ray
09-15-2008, 07:36 PM
I had been practicing variations since 1995 and my sister since 1968 (dry sifts). A second run only produced minimal amounts, not economically feasible in man hours. Our average run of 116 grams of plant material generally produced 4 to 9 g of extract, dependent on bract ratio.

sounds like it worked then, still it would be nice to see pics or perhaps I can replicate to see for myself



Where did you get this information?

from studying essential oils, there is lots of info out there... I will see what I can dig up
a simple test would be to make bubble then look at the water and see the essential oils floating on the water, which if left on the water for a day or so will become rancid etc...if I was to put some bubble in a glass of water and shake I'd guess that essential oils would separate from the bubble and become degraded and otherwise lost to the process

I've attached a document you may have already seen. I've read another and thought I'd saved it but can't locate. I'll keep looking.

that is an interesting doc thanks, I skimmed it but will read it later

c-ray
09-15-2008, 08:06 PM
I should also point out that I prefer to use fresh material (freshly harvested from plants) that is frozen for at least 1/2 hour, as per the usual bubbleman methodology, as there is the highest quantity of essential oils still present in the material and since essential oils have huge healing properties it is important to make sure they are present in the highest quality and quantity possible

in the drying process essential oils are lost to the air, reducing the medicinal qualities of the bubble hash

c-ray
09-15-2008, 08:08 PM
from http://www.foodproductdesign.com/articles/463/463_1095AP.html

Essential oils are also subject to oxidation. This reduces the shelf life of the flavor itself and the flavor of certain confectionery products. While a glassy hard candy matrix largely protects the essential oil from exposure to oxygen, others do not. Marshmallows, creams and other aerated products incorporate air, exposing susceptible flavors to oxygen. Oxidation of essential oils tends to result in typical soapy notes. Citrus essential oils are particularly subject to oxidation and the formation of terpenes.

"This is one of the most critical stability issues in the flavor industry," notes Birgit Mitsch, business unit director, confectionery group, Firmenich, Princeton, NJ. "When a citrus flavor becomes oxidized, it develops objectionable off-notes in the flavor and in the finished product. Because of this, a standard citrus liquid or powder flavor has a shelf life of only one year. Certain encapsulation processes can protect flavors from oxidation."

Bram
09-21-2008, 06:31 AM
i needs to get me a hippie to do the mixin!

:ciao:

vapor
09-22-2008, 12:10 AM
if you not busy plan on a few daze and that would be fine eh.,.,^^

guest
09-22-2008, 03:30 AM
Fascinating c-ray.

guest
09-25-2008, 06:46 PM
I vote for a motion to co-ax C-ray into starting a kick-ass Terpenes FAQ and research Thread!
Who is with me?
TD

c-ray
09-26-2008, 08:03 AM
ha ha ha! :laugh2:

nuggdigger
03-20-2011, 07:55 PM
one bag of ice
in went the trash
topped 2/3 with fresh snow scooped off the trampoline,
mixer'up
shaker'up

next to be placed in the used bathtub water for the meltdown

thanxmon:rasta2:

peace